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target="_blank">甲酸?/a>的用,一直以来便是备受关注的Q对它,我们在前面也提到刎ͼ它与甲酸有着密不可分的联p,q让不少惛_Q甲酸是否可以制成甲酔R?大家认ؓ?有的为是可以的,有的人则持有相反的想法,I竟l果是怎样的呢Q让我们一起去看看吧?br />   ?12g酸钠加热溶?L水中Q往此水溶液中加入少量甲酸水溶液Q此Ӟ在生成甲酔R沉淀的同时可使其中的杂质与其共沉淀而除厅R再?52g_ֈ的甲酸,溶于1L热水(90?中,在烧杯中Q预先将500mL水热?0℃,在搅拌下Q用分液漏斗甲酸和酸钠水溶液{体U的慢慢滴入烧杯中,此过E应保持溶液的pHgؓ6?。滴毕,再稍加热后,冷却此溶液ƈ滤出生成的结Ӟ用冷水洗涤,晶体?40?50℃下q燥Q再|于硫酸的q燥器中?br />   它的_ֈ依上法制得的或市售的甲酸钠可用水重结晶纯化。先用热水溶解,在约90℃下辑ֈ饱和Q趁热抽滤,再往滤液中加?5%(体积分数)的乙醇水溶液Q放|冷_滤出晶体Q在250℃下q燥。由于它水溶液能与玻璃器皿发生反应,也因为原料中含有杂质Q产品中含有二氯化和酸钠,制备操作应注意尽快操作,也可用精制的氢氧化钠代替酸钠。此外,在制备它Ӟ如溶液偏酸性,会生成微量甲酸氢钠,与其共沉淀析出Q品如?50?00℃下q燥Q甲酸氢钠即可发生热分解而成酸钠?br /> <div> <br /> </div> </div> <div class="fanhui"></div> <div class="NewsView-title-Share"> <!-- Baidu Button BEGIN --> <div id="bdshare" class="bdshare_t bds_tools_32 get-codes-bdshare"> <a class="bds_qzone" title="分n到QQI间" href="#"></a> <a class="bds_tsina" title="分n到新微? href="#"></a> <a class="bds_tqq" title="分n到腾讯微? href="#"></a> <a class="bds_renren" title="分nCh人网" href="#"></a> <span class="bds_more">更多</span> <a 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